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Category : Bioscience, biotechnology, life health science (precision equipment, instruments, devices and accessories) > Liquid handling equipment, dispensers, pipetting
Liquid-Liquid Extraction Pilot Mp1030 - Deltalab
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The liquid-liquid extraction is achieved by feeding the top and the bottom of the column respectively with the heavy and light phases by means of a pump. This procedure consists in bringing a feed solute into contact with a more akin solvent. The extraction column is provided with a stirrer throughout its length. The stirrer is powered by a variable speed motor. At the top of the column, an azeotropic separator provides the separation of the two phases. - Determination of the transfer units - Height of a unit of transfer - Efficiency of extraction - Mass balance - Calculation of the material exchange coefficient - Calculation of the theoretic number of stages - Concentration profile in the column - Practices on a system with three partially miscible components : Acetic acid – toluene – water Acetic acid – isopropyl ether – water Acetic acid – ethyl acetate – water - Extraction column DN 50, in borosilicate glass, H = 600 mm - 1 Disk stirrer, stainless steel AISI 316 execution variable speed reducer 0-800 rpm - power 300 W - 2 decanters DN 100, in borosilicate glass - 4 tanks in polythene, capacity : 30 l ( 2 for feeding and 2 for the refined and extracted product ) - 2 gear pumps with manual control, stainless steel body AISI 316, flow range 0- 40 l/h with check valve - Speed driver with display - Solvent flowmeter, in stainless steel and glass, scale : 4 to 40 l/h - Solution flowmeter, in stainless steel and glass, scale : 4 to 40 l/h - Electric cabinet, IP 55, with transformers, start/stop switch, emergency stop, security device and synoptic. - Technical manual 1800 x 800 x 2000 mm Power supply : 220 V - 50 Hz
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